April 07, 2004
By: Tannis Alder
Website: http://www.1st-in-wellness.com
Testing verifies technique for analyzing taste & odor-causing agents
A new, three-step technique for detecting taste and odor sources in bottled
water has been shown effective in identifying and quantifying the agents at fault, down to the
low parts per billion level. Verified by recent testing and confirmed in a blind study by a panel
of judges, the process involves three exacting laboratory test methods to isolate, identify, and
measure taste- and odor-causing components.
This approach gives us a reliable way to find the problematic compounds, using a series of
proven test methods, said Gary Deborski, Market Development Manager for Impact Analytical.
The combination gives us an excellent basis for making judgments on the sources of
contamination and how to eliminate them.
With staff members having as much as 35 years experience in taste and odor testing, the
company is one of just a few analytical labs in the country with the expertise to not only generate
test data, but also offer complex analysis, draw detailed conclusions and make recommendations
for problem-solving.
Two of our biggest strengths in plastics processing are taste/odor analysis and additives
analysis, commented Deborski. Taste and odor are critical in food and beverage products, and
we’ve developed many techniques for identifying and resolving those issues, including an
experienced taste and odor test panel, he said.
The bottled water market represents big business, by any standard.
According to the Natural
Resources Defense Council, over half of all Americans drink bottled water, with more than a
third of those indulging more than once a week. The NRDC reports that sales have nearly tripled
in the last decade, with U.S. sales currently in excess of $4 billion. Globally, the market was
estimated to be worth $14 billion at the wholesale level in the late 1990s, and it’s grown at a rate
of about 8% each year since then, nearly twice as fast as other beverages.
Bottled water sellers rely heavily on their image of purity to market their products, which are
perceived to be safer and of higher quality than tap water. Some consumers also report
switching to bottled water because they find the taste and smell of tap water offensive. In both
cases, avoiding undesirable taste- or odor-causing components is essential.
Test methods
Overcoming taste and odor problems in bottled water requires analytical methodology capable
of characterizing materials down to extremely low concentrations, explained Eric Hill, taste and
odor chemist. Any component contributing even a small effect is likely to be apparent in water,
even if it might pass completely unnoticed in flavored beverages.
To verify the new test regimen, scientists at Impact Analytical first conducted steam
distillation/extraction on each packaging component of their store-bought samples of bottle
water, which was reported as having an off-taste by a five-member panel. They followed with a
class separation to isolate and identify the problem components. During this stage, a process
known as capillary gas chromatography/mass spectrometry is also used to identify
oxidation products commonly formed during package fabrication, which could contribute to taste
and odor.
The second part of the test sequence involves reverse-phase high performance liquid
chromatography or HPLC, along with a UV detection system to gauge additive levels in the
packaging materials. During this step, extracts of the bulk material are also analyzed by HPLC
and GC/MS to further test for any additives and oxidation products.
The final stage is analyzing the packaged water itself for insights into the taste / odor source.
Impact Analytical chemists perform an extraction on large quantities of the packaged water,
trapping foreign substances and analyzing the resulting absorbent via thermal desorption-
GC/MS to find any hydrophilic components that may be present. Taken together, these methods
serve as a powerful tool for experienced researchers to identify problem compounds and possible
sources, as well as make recommendations for their elimination.
With considerable resources in polymer science, Impact Analytical will highlight its resident
expertise in process engineering, packaging and materials testing this summer at NPE, the
world’s largest plastics and elastomers trade show. Sponsored by the Society of the Plastics
Industry, the triennial event will be held at McCormick Place in Chicago, the
largest exposition facility in North America.
Since 1971, Impact Analytical has delivered extensive problem-solving capabilities, detailed
analysis and method development to customers in plastics manufacturing and processing.
The
company’s experienced technical staff provides characterization of unknown materials,
permeability testing, competitive product analysis, identification of impurities, investigation of
product failures and supplier certification.
About
The Author:
Tannis Alder is a successful author and regular contributor to http://www.1st-in-wellness.com.
Obtaining and keeping good health through healthy living, natural healing, great mental health and healthy finances.